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To avoid amorphisation of the sample during grinding, wet milling is done in a McCrone Micronizing mill. Before grinding in the McCrone Mill, the samples are crushed and passed through a 500 micron sieve. Take representative amounts of sample (50-100 g). Crush the sample by hand in a porcelain mortar. Use shock impact for grinding, avoid shearing.

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The McCrone Micronizing Mill was designed to reduce a few grams of material to micrometer size particles of a narrow size range, minimizing contamination, time, cost, and mess. What kind of grinder is it? It is a vibratory laboratory mill powered by a 1/30 HP motor. The

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By the help of Dr. Lieven MACHIELS from KuLeuven, it is reported in his doctor thesis that several authors have shown that wet grinding using a McCrone Micronizing mill is the most efficient method of reducing the particle size of most materials, while avoiding many of the deleterious effects that can be associated with mechanical grinding (O ...

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